Chemical Review and Letters

Highly sensitive determination of nimesulide using Glassy Carbon Electrode Enhanced Graphene Oxide-Multi-walled Carbon Nanotubes

Document Type : Review Article

Authors

Adil Rashak 1
Faiq F Karam 2

1 Chemistry,science, university of AL-Qadisiyah, Diwaniyah, Iraq

2 Department of chemistry-College of Science-University of Al-Qadisiyah , Iraq

https://doi.org/10.22034/crl.2024.469494.1390
Abstract
Methods: NIM was determined utilizing (GO-MWCNTs/GCE) using DPV. The impact of different experimental factors, such as scan rate, pH, and aggregation time, on the voltammetric responses of NIM was assessed.

Results: NIM achieved an irreversible electrochemical reaction controlled by the diffusion-controlled electrode method at GO-MWCNTS/GCE. This research examined the relationship between peak oxidation current and concentration under optimal conditions. A calibration curve was plotted showing the linear range of 0.06-0.8 ppm and limited of detection of 0.000318 ppm. The approach was effectively used to detect NIM in drugs as well as in human serum and urine samples. Results refer that the chosen method is fast, responsive, and cost-effective. The sensor (GO-MWCNTs/GCE) had an excellent reproducibility and good repeatability.

Keywords

Nimesulide
GO-MWCNTs
Glassy Carbon Electrode
CV
DPV

Subjects

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Chemical Review and Letters
Volume 7, Issue 4 - Serial Number 4
September and October 2024
Pages 719-730

  • Receive Date 24 July 2024
  • Revise Date 12 August 2024
  • Accept Date 23 August 2024

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